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International Journal of Energetic Materials and Chemical Propulsion
ESCI SJR: 0.149 SNIP: 0.16 CiteScore™: 0.29

ISSN Print: 2150-766X
ISSN Online: 2150-7678

International Journal of Energetic Materials and Chemical Propulsion

DOI: 10.1615/IntJEnergeticMaterialsChemProp.2013008463
pages 1-6

SYNTHESIS OF 3-AZIDO-1,2,4-TRIAZOLIUM 5,5'-AZOTETRAZOLATE

Kirstin F. Warner
Naval Surface Warfare Center, Explosive Ordnance Disposal Technology Division, Indian Head, MD 20640
Victor J. Bellitto
Naval Surface Warfare Center, Explosive Ordnance Disposal Technology Division, Indian Head, MD 20640
Richard H. Granholm
Naval Surface Warfare Center, Explosive Ordnance Disposal Technology Division, Indian Head, MD 20640

ABSTRACT

The synthesis of 3-azido-1,2,4-triazolium 5,5'-azotetrazolate is described. The physical and explosive sensitivity properties of this material were determined. This salt was characterized by nuclear magnetic resonance, infrared spectroscopy, and X-ray photoelectron spectroscopy. Thermal properties were studied by differential scanning calorimetry (DSC). The reaction to mechanical stimuli was also determined by small-scale sensitivity testing, small-scale shock reactivity testing, and small-scale internal blast testing.


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